Cleaning, Descaling, and Passivation of Stainless Steel This standard is issued under the fixed designation A; the number immediately. Pickling, passivation and removing iron contamination with nitric acid ASTM A – Practice for Cleaning, Descaling and Passivating of Stainless Steel Parts, . Passivation per ASTM A Posted on November 29, Latest News. APT to Exhibit at SHOT Show in Las Vegas, NV. Advanced Plating.
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We’ve been in the metal finishing business for over 80 years.
ASTM A380 Passivation Standard
While the practice provides recommendations and information concerning the use of acids and other cleaning and descaling agents, it cannot encompass detailed cleaning procedures for specific types of equipment or installations. Precaution shall always be practiced to minimize iron contamination, in reuse of cleaning and pickling solution, in water rinsing, in circulation of cleaning solutions and rinse water, in protection of cleaned surfaces, for safety, and disposal of used solutions and water.
All information presented is for general reference and does not represent a professional opinion nor the policy of an author’s employer. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. The following shall be used as the basis for cleanness acceptability: Stainless steels cannot be passivated unless the steel surface is clean and free from contamination and scale from welding operations.
The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Although cannot see the reason obviously myself? This ensures that the surface of the workpiece is free of scale and contaminates.
Stainless steels are designed to naturally self-passivate whenever a clean surface is exposed to an environment that can provide enough oxygen to form the chromium rich oxide surface layer, on which the corrosion resistance of these alloys depends.
To my knowledge it is not possible to do a combination pickling and passivation. In order to avoid ambiguity in the setting of requirements, it may be necessary for the purchaser to define precisely the intended meaning of passivation.
Meaningful tests to establish the degree of cleanness of a surface are few, and those are often difficult to administer and to evaluate objectively. This process greatly reduces the formation rust on the surface of the workpiece.
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For more specific safety precautions see 7. Citric acid is a less hazardous method and has environmental benefits in terms of ‘NOx’ fume emission and waste acid disposal. Visual inspection is suitable for the detection of gross contamination, scale, rust, and particulates, but may not reveal the presence of thin films of oil or residual chemical films.
Having been in the metal finishing industry for nearly a century, Keystone Corporation meets the qualified standards of ASTM A and is well qualified to handle your passivation needs. If you let this solution inside your S. This formula should not hurt your electropolished surfaces. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Unless otherwise specified, it is this definition of passivation that is taken as the meaning of a specified requirement for passivation.
Give us a call or visit our contact page to request a quote for your project today! In some cases, no more than degreasing or removal of gross contamination is necessary.
Scales shall be removed through chemical descaling, acid astn, and mechanical descaling.
It’s not possible to diagnose a finishing problem or the hazards of an operation via these pages. Historical Version s – view previous versions of standard. Recommended cleaning practices shall be followed for welds and weld-joint areas, specially critical applications, installed systems and post-erections.
This would attack electro-polished surfaces and is not the kindest way to treat them. The selection of procedures from this practice to be applied to the parts may be specified upon agreement between the supplier and the purchaser. Let us know if we can help. The standard notes that the high carbon martensitic stainless steels, such as C, are not suitable for acid passivation as they can be attacked or be subject to hydrogen embrittlement.
Keystone Corporation is an industry leader in the passivation of stainless steel. Some of the various meanings associated with the term passivation that are in common usage include the following:. Precision inspection shall be performed by solvent-ring test, black light inspection, atomizer test, and ferroxyl test.
Although they apply primarily to materials in the composition ranges of the austenitic, ferritic, martensitic, and duplex stainless steels, the practices described may also be useful for cleaning other metals if due consideration is given to corrosion and possible metallurgical effects.
I am not sure exactly what you want to do, but the atm formulations can give you increased performance over the old nitric formulations.
Lee Kremer Stellar Solutions, Inc.
Passivation of L SS per ASTM A
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Passivation often follows the process of pickling. This practice covers the standard recommendations and precautions for cleaning, descaling, and passivating of new stainless steel parts, assemblies, equipment, and installed systems.
The standard also allows any combination of citric acid concentration, temperature and time, provided that the passivation test criteria can be met. Such chemical treatment is generally not necessary for the formation of the passive metal oxide film. Related Links Suppliers of Passivating Products. It was at one time considered that an oxidizing treatment was necessary to establish this passive metal oxide film, but it is now accepted that this film will form spontaneously in an oxygen-containing environment providing that the surface has been thoroughly cleaned or descaled.
Consideration shall be given in the design of parts, equipment, and systems that will require cleaning to minimize the presence of areas in which dirt, or cleaning solutions might become trapped, and to provide for effective circulation and removal of cleaning solutions. Process Class Stainless Steel Types C1 or C2 Austenitics, austenitic precipitation hardening and duplex C3 High chromium martensitics C4 Ferritics, martensitics and martensitic precipitation hardening.
Unlike ASTM A, the standard does not require specific solutions for particular stainless steel grades or types, although 3 specific treatments are identified.
These recommendations are presented as procedures for guidance when it is recognized that for a particular service it is desired to remove surface contaminants that may impair the normal corrosion resistance, or result in the later contamination of the particular stainless steel grade, or asgm product contamination.
For certain exceptional applications, additional requirements which are not covered by this practice may be specified upon agreement between the supplier and the purchaser.
Citric acid passivation as an alternative to nitric acid asstm Citric padsivation treatments can also be considered as an alternative to nitric acid as both provide the oxidising conditions necessary for passivation.
The treatments are then defined by the process classes. Pickling, passivation and removing iron contamination with nitric acid Passivation treatments are sometimes specified, but it is important to consider whether this is strictly necessary or not.
I believe you must pickle the spools with an acid which contains fluoride in some form — often a standard nitric-hydrofluoric pickling acid or pickling paste, and follow this either with electropolishing or with passivaation acid passivation or citric acid passivation to the standards discussed above. Some of the various meanings associated with the term passivation that are in common usage include the following: